Indian Council of Agricultural Research
(Agricultural Knowledge Management Information System)


ICAR-Directorate of Groundnut Research, Ivnagar Road, P.B.No.5, Junagadh-362001 Gujarat (www.dgr.org.in)
Click Here to See Management Committee
Instrument Details
Instrument/Facility Name: Nitrogen Analyser
Make                                   : LECO Corporation, USA
Model                                  : FP 528
Specification   :Readability: 0.001%, Calibration: Standard Sample; Linear, Analysis Time: 3 minutes, Sample Size: Up to 250 mg, Detection Method: Thermal Conductivity, Furnace Range: Up to 975o Celsius

Click to View1. Instrument Range Helium Model (3 cc Aliquot Loop): 0.04 mg to 250 mg absolute Nitrogen Argon Model (10 cc Aliquot Loop): 0.1 mg to 100 mg absolute Nitrogen 2. Precision Helium Model (3 cc Aliquot Loop): 0.02 mg or 0.5% RSD, whichever is greater Argon Model (10 cc Aliquot Loop): 0.05 mg or 1.0% RSD, whichever is greater 3. Readability: 0.001% 4. Calibration: Standard Sample; Linear 5. Analysis Time: 3 minutes 6. Sample Size: Up to 250 mg 7. Detection Method: Thermal Conductivity 8. Chemical Reagents: Anhydrous Magnesium Perchlorate, Calcium Oxide, Sodium Hydroxide on an inert base, Copper Sticks, N Catalyst Reagent, Copper Turnings, Alumina Pellets, Magnesium Oxide 9. Gas Required Carrier Gas: 99.99% Helium or Argon, 40 psi (2.8 bar), ±10% , Combustion Gas: 99.99% Oxygen, 40 psi (2.8 bar), ±10% Pneumatic Gas: Compressed Air, 40 psi (2.8 bar), ±10%. 10. Gas Flow Rates Carrier Gas: Analysis 200 mL/min (measure), 30 mL/min (reference), Conservation: 30 mL/min (measure), 30 mL/min (reference), Combustion Gas: 1.3 to 6 L/min (user programmable oxygen profile) 11. Furnace Range: Up to 975o Celsius 12. Electrical Power Requirements: 230 V~ (±10%; at max load), 50/60 Hz, single phase, 10 A, 7,900 BTU/hr

  Working Principles
Click to ViewThe sample were placed into a hot furnace and flushed with pure oxygen for very rapid combustion, where by nitrogen containing material is converted to molecular nitrogen and the by-products of combustion (CO2, H2O, NOx, and N2) pass through the furnace filter and thermoelectric cooler for subsequent collection in a ballast apparatus. These collected gases in the ballast are mixed, and a small aliquot dose is then used for further conversion of the gases. The remaining aliquot that has been reduced is measured by the thermal conductivity cell for Nitrogen.

  Applications
  User Instructions
1. Used for the estimation of total nitrogen present in the sample. 2. Nitrogen/Protein analyser is an alternative method of Kjeldahl. 1. Sample should be preferably submitted in pulverized form. 2. Sample requirement: 2-5 g

  Contact Us
Contact No. +91-9725018784
Email Id maheshmahatma@gmail.com

  Nitrogen Analyser Charges
Procedure Name
Industry
University
National LAB/R&D
Remark
Standardization & Estimation
1000
400
500
Per Sample,(Rs.) including GST
Subsequent Sample estimation
800
200
300
Per Sample,(Rs.) including GST
Sample preparation
200
50
100
Per Sample,(Rs.) including GST

Additional Rs 100/-towards postal charges if result are to be posted
The Demand Draft should be in favour of "ICAR-Directorate of Groundnut Research, Junagadh OR Electronic transfer to ICAR-Directorate of Groundnut Research, Junagadh (ACC No: 10283132519 IFSC Code: SBIN0003251)"
Letter, DD & Samples send to "Director, ICAR-Directorate of Groundnut Research, PB 5, Junagadh, Gujarat, India-362001"